Fmoc spps
α-N-Heterocyclic Thiosemicarbazone Derivatives as ...
The standard SPPS procedure is applied with Fmoc/t-Bu protecting group scheme and using 4-(4,6-dimethoxy-1,3,5-triazin-2-yl)-4-methylmorpholinium toluene-4-sulfonate (DMT/NMM/Tos-) [49] or 4-(4,6 ...
[DOCX File]Welcome to CaltechAUTHORS - CaltechAUTHORS
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Bulk synthesis of PCC candidates was carried out on 2-chlorotrityl chloride (CTC) resin (1.04 mmol/g) using microwave-assisted Fmoc-based solid-phase peptide synthesis (SPPS). The first amino acid was attached to the resin following the vendor’s protocol. The resin was transferred to the CEM Liberty 1 for the coupling of the remaining amino ...
[DOCX File]Lecture 1: Key Concepts in Stereoselective Synthesis
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The development of SPPS by Merrifield revolutionized the field of peptide chemistry. Today, SPPS is acknowledged as the method of choice for creating peptides in a synthetic manner. In the most common strategy the C-terminus of an amino acid (with protected side chain and N-terminus) is immobilized on a solid support (e.g. cross-linked ...
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Fmoc-based solid phase peptide syntheses (SPPS) were carried out on a Prelude synthesizer from Protein Technologies. Standard side-chain protecting groups were used: Arg(Pbf), Asn(Trt), Asp(O t
[DOCX File]Scitation - AIP Publishing
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The biotin was coupled into the N-terminus of assembly peptide with SPPS method using the assembly peptide before cleavage of peptides from resin, the SPPS method, a microwave peptide synthesizer, and Fmoc chemistry. The crude products were cleaved from H-rink Amide-ChemMatrix® resin (0.53 mmol/g, PCAS) in the solution of trifluoroacetic acid ...
[DOCX File]www.peptide-soc.jp
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Fmoc-based SPPS, HTLV-1 protease, hydroxyethylamine isoster, Inhibitor, Retro-inverso peptide. Introduction. Human T-cell leukemia virus type 1 (HTLV-1) is a retrovirus which cause adult T-cell leukemia (ATL) and related diseases. The key enzyme in the processing of virus proteins in the HTLV-1 is an aspartic protease called HTLV-1 protease.
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All peptides were prepared by Fmoc SPPS methods using Rink amide resin with an initial loading of 0.61 mmol/g, unless otherwise noted. Resins were swollen in N,N-dimethylforamide (DMF) for 45 min prior to synthesis. For sequence extension, the Fmoc-Arg(Pbf)-OH (5 eq.) was activated by treatment with 1-O-Benzotriazole-N,N,N’,N’-tetramethyl ...
[DOCX File]Normal.dot - Osteoarthritis
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Fmoc-O2Oc-OH was coupled as a spacer to peptides subjected to FITC modification. FITC-labelling was performed twice with a 4-fold excess of FITC Isomer I and 8 eq. DIPEA in NMP for 1 h. Peptides were cleaved from the resin with TFA/H2O/TIPS (95/2.5/2.5) for 4 h and precipitated with diethyl ether at -20_C. Semi preparative HPLC was carried out ...
[DOCX File]Centers for Disease Control and Prevention
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were synthesized using SPPS by attaching Fmoc-Gly-OH to the Rink amide, by first removing the 9-fluorenylmethoxycarbonyl (Fmoc) protecting group using a 20% solution of piperidine in dimethylformamide (DMF, 2 x 8 min). The resin was subsequently washed three times in DMF (3 x 5 min) prior to coupling the amino functionality of the resin to Fmoc ...
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