Ir and mass spec practice

    • [DOC File]Good Laboratory Practice in Analytical Laboratory

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      As IR-4 lab practice, residue levels in the untreated control samples should be less than LLMV (lowest level of method validation). ... liquid chromatography system for good laboratory practice level quantitative analysis by liquid chromatography/tandem mass spectrometry. Rapid Comm Mass Spec 2002;16 (1):43-52.


    • [DOC File]Treenascool

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      Model answer practice test THREE (C) From the IR spectrum: Presence of a medium peak at 600-700 cm-1 indicative of a Br or a Cl group. Absence of a strong, sharp peak resulting from a C=O stretch at 1810 – 1775 cm-1 (1700cm-1) indicates no carbonyl group, therefore not …


    • [DOC File]Mass Spec and IR - Iowa State University

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      What is the x-axis of an IR spectrum and what are its units? Wavenumber, in cm-1. Draw the bond which gives the following IR absorptions: 1100 cm-1 (C-O) 1700 cm-1 (C=O) 3500 cm-1 (O-H) Which of the following are the expected products of the cleavage of 2-pentanone (shown here) in mass spec?


    • [DOC File]Treenascool

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      From the IR spectrum: Absence of a strong, sharp peak resulting from a C=O stretch at 1700cm-1 indicates no carbonyl group, therefore not butanoic acid or methyl propanoic acid. Presence of a broad strong peak at 3300-3600 cm-1 resulting from an OH stretch indicates an OH group therefore supports the other 2 molecules. From the Mass Spec:


    • [DOC File]CHE 235 Unit 1 - Chemistry Solutions

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      The unit introduces the study of chemical reactions by use of mechanisms, kinetics, and thermodynamics. Also covered in this unit are the techniques of IR and Mass Spec as used in the structural determination of organic compounds and identification of unknown compounds. B. Topics: 1. …


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